Training for faculties

AEI-2151302 Term Date:19-06-2017 to 13-10-2017

Dear students, 

       Welcome to the new semester!

      I look forward to working with you over the next some weeks in  ADVANCED ENVIRONMENTAL INSTRUMENTATION (2151302). Get ready for a journey of a lifetime learning memories. In this class you will learn about instrumental method of chemical and pollutant analysis by optical and/or electro-analytic techniques. Some of the instruments like GC, FTIR, Spectrophotometer, TOC and many more. More over this, we will learn some research oriented and statistical data analysis methods too. These will be useful to your shining carrier in the field of environmental science and engineering. 

Assignment:-1			Suggested Marks
What is Advanced Environmental Instrumentation? What is its Importance?	7
Explain the mechanism of environmental analysis	7
Write about steps of environmental analysis process	4
Give the classification of analytical methods of analysis.	7
What is the role of environmental chemist?	4
What is Electromagnetic spectrum? Explain in detail.	5
Describe the Lambert and Beer laws of light absorption	7
Explain visual colorimetry in detail.	7
Write about instrumentation and workings of UV-Visible  spectrophotometry	7
Differentiate between spectrophotometry and colorimetry	7
Assignment:-2
Explain Working principle of Flame photometer. Which parameters can be measured using flame photometer?		7
Give the difference between Raman Spectroscopy and Infrared Spectroscopy.		7
Write a short note on Mass Spectroscopy.		5
Explain Atomic Adsorption Spectroscopy in detail.		5
Differentiate following molecules based on IR-spectroscopy		4
Explain in brief the importance of “Mutual exclusion rule” for the IR &Raman spectroscopy with two examples.		3
Draw the schematic diagram of Raman-Spectrometer and describe each part in detail.		7
Write note on infrared spectroscopy		7
Write a note on atomic spectroscopy		5
Write the two application of followings: (1)UV-Visible spectroscopy(II)Infrared spectroscopy (III) Gas chromatography		6
Assignment:-3
Write the sources of Turbidity in river water. What is significance of turbidity? And methods of determination.		7
Write a short note on Nephelo Turbidity Meter.		7
Give the difference between visible and instrumental method for measurement of turbidity.		4
Explain “Jackson Candle Turbidity Meter” with neat sketch.		7
Write application of turbidity data and its standard unit.		5
What is Chromatography? Explain stationary phase in Chromatography		7
Explain the working principle and operation of each unit of High Performance Liquid Chromatograph with sketch.		7
Give the applications of High Performance Liquid Chromatography.		3
Explain the working principle and operation of each unit of gas chromatograph with sketch. Along with its merits and demerits.		7
What is chromatography? Give the difference between stationary phase and mobile phase in chromatography		7
Assignment:-4
Give the difference between adsorption and partition chromatography with examples.		5
Write the short note on “Affinity in chromatography”		3
Explain the principle of Ion Chromatography(IC) in detail		4
Explain following terminology use in chromatography 1.Normal phase 2.Reverse phase 3.Retention time 4.Retention volume 5.Relative retention 6.Column efficiency 7.Resolution		7
Explain stationary phase in Chromatography.		3
Mention the classification of chromatography and write note on column chromatography		7
Write a note on ion –exchange chromatography		7
Write a note on thin layer chromatography		5
Explain the significance of chromatography in a method of analysis		4

LIST OF PRACTICALS

NO	TOPIC	Page No.	DATE	GRADE	SIGN
	Safety Test and Safety Symbols
1	Determination of the turbidity in the given samples.
2	Determination of fluoride concentration in drinking water using spectrophotometer.
3	Colorimetric analysis for copper using UV-Vis spectrophotometer.
4	Preparation of calibration curve of chromium using UV- Vis spectrophotometer.
5	Determination of metals (chromium/nickel/copper/arsenic) using Atomic Absorption Spectrophotometer
6	Determination of cations and anions using Ion-Chromatograph
7	Determination of TOC from wastewater using TOC analyzer

Assignments

Sr. No	Assignments no. / Unit	Expected Date	Submission Date	Grade		Faculty Sign
1	Assignment:1	17-07-2017
2	Assignment:2	01-08-2017
3	Assignment:3	19-08-2017
4	Assignment:4	04-09-2017
5	Assignment:5	10-10-2017

Open Ended Project

Sr. No	Open Ended Project Topic	Date of submission	Submission Date	Grade	Faculty Sign
1		01-10-2017
Enroll no.(s) Of Partner if any

Word file

Sr. No	Topic of MS-Word file	Date of submission	Submission Date	Grade	Faculty Sign
1		15-07-2017

PPT file

Sr. No	Topic of MS-PPT file	Expected Date	Submission Date	Grade	Faculty Sign
1		21-07-2017

All PPT and word file must be sent  on the email: aeibrsudani@gmail.com only.

 File name must be 150190113xxx_topic name.doc or 150190113xxx_topic name.ppt    check it before you send.

Organic Chemistry And Unit Processes (2130501) Term Starts on 12-06-2017.

To all our new and old students.
       Welcome to the new semester!

      I look forward to working with you over the next 19 weeks in  OC&UP(2131301). Get ready for a journey of a lifetime learning memories. In this course you will learn about general organic chemistry and unit processes Stereochemistry, Petroleum Chemistry, Colour,  Dyes and Pigments and many more topics which will help you to gain a vast knowledge regarding basic chemistry behind the synthesis of chemical. in addition to this some topics like, Synthetic Drugs, Amino acid & Protein Chemistry and  Hetero-cyclic Compounds will also guide you to get required knowledge regarding the emerging and developing field of biochemical engineering.

Weekly participation in 3 lectures and one laboratory of 2 hours are essential throughout the course to be successful in the subject.

This course will have 7 Laboratory based experiments, 5 Assignments, One power point presentation, One active learning assignment in MS-Word file, one question bank preparation assignment, one 'Open Ended Project' work. And one 'Online Test'.

We hope that, once more it will a good and interesting course program for you. Even though we have tried to finalize our scheduling and class rooms allocations, Class room and time changes may occur. Therefore, we would like to ask you to frequently check our notice boards for notifications and updates. It is also advised to visit this blog frequently for getting new learning experiences, learning materials or some instructions.

Assignment:0 Prerequisite 

1.            Write 50 IUPAC names of organic molecules and draw their structures.

2.             Draw 50 structures of organic molecules and write their IUPAC names. 

Assignment:1 

1.       Differentiate fission and fusion reaction with two examples.

2.       Define the terms: Free Radical, Carbonium, Carbanion, Carbenes and Nitrenes. Nucleophilles and 

          Electrophilles with suitable example and figure.

3.       What are SN1 and SN2 reactions explain with examples one of each.

4.       Describe four main types of organic reactions.

5.       Explain the manufacturing process of Acetic acid

6.       Explain mechanism of   Esterification with an example.

7.       Discuss Strengths of Acids.

8.       Explain the nomenclature of carboxylic acids. 

9.      Give manufacturing process of following acids : Formic acid, Oxalic acid, Palmitic acid & Stearic acid with suitable illustrations. 

Assignment:2

1.            Define Optical, Geometrical and Conformational Isomerism with proper examples.

2.             What is call optical activity with respect to organic compounds?

3.            Explain Polarimeter with its instrumentation, working and importance.

4.            Define specific rotation with importance.

5.            Explain the concept of Diasteromers, Enantiomers and meso compound with the example of lactic acid and tartaric acid.

6.            Explain E and Z designation with two examples.

7.            How would you carried out Resolution of (i) racemic mixture of acids and (ii) racemic mixture of bases?

8.            Differentiate between unit process and unit operation Discuss the advantages of continuous process and batch process over each other.

9.            Finde out the absolute configuration of followings.

10.           Define nitration. Enlist various nitrating agents and discuss the function of sulphuric acid in the mixed acid used for nitration

11.           Describe the batch nitration of benzene with mixed acid Give an account on methods of reduction for the preparation of amines. Illustrate various products of reduction of nitrobenzene

12.           Explain kinetics and mechanism of aromatic nitration. What is the        effect of Nitrous acid on nitration

13.           Describe the manufacture of p – nitro acetanilide Define unit process. Why is it so called? How do unit processes differ from unit operation?

14.           Give a brief account of nitration of paraffinic hydrocarbon Give evidence to establish the formation of nitryl ions in a nitration process conducted using mixed acids

15.           Describe following unit processes –with suitable industrial important chemicals: Amination, Hydrogenation, Halogenations, Oxidation and Reduction.

16.          Explain following unit processes –with suitable industrial important chemicals: Sulphonation, Hydrolysis, Alkylation and Polymerization.

Assignment:3 

1.            What is polynuclear compound. Write preparation, properties and uses of Naphthalene, 

2.            write structural formula of anthracene and  give one preparation and three reactions.

3.            What is heterocyclic compound? give synthesis and reactions of pyrrole and Furan.

4.            Write about nomenclature of heterocyclic comppounds.

5.            Give one synthesis and two uses of each: Thiophene, Pyridine and Quinoline.

6.            Write about the chemical properties of Thiophene, Pyridine and Quinoline.

7.            Compare the physical properties of Thiophene, Pyridine and Quinoline, Furan, Naphthalene, Anthracene.

8.            Explain the term carbohydrates. And give classification.

9.            Give two chemical reactions of each: Glucose, Fructose and Starch.

10.          Give the conversion of any aldose to ketose and ketose to aldose.

11.          Give conversion of pentose to hexasose.

12.          Explain the manring of cane sugar from sugarcane with flow sheet.

Assignment:4

1.            Define the terms i) Aminoacid ii) alpha amino acid iii) Protien

2.            Prepare a note on  qualitative tests of proteins.

3.            Give any three synthesis of aminoacids.

4.            Give properties of aminoacids.

5.            What is amphoteric nature of amino acid?

6.            explain isoelectric point.

7.            Prepare a note on Primary, Secondary, Tertiary and Quartanery Structure of Protein.

8.            What are RNA and DNA. give types of RNA.

9.            Explain the importance of DNA and its structure.

10.          Write mechanism and four uses of these reactions: Canninzaro, Wolf Kishner and Clasien.

11.          What is call diazotisation? Explain with importance in different chemical manufacturing.

12.          Explain sandmayer reaction with mechanism.

13.          Compile some facts like General reaction, Mechanism, examples and applications on Curtius reaction.

14.          What is Baeyer Villiger oxidation reaction? Give mechanism and application.

15.          Give some applications of Hoffman degradation reaction with any one mechanism .

16.          Prepare a note with General reaction, Mechanism, examples and applications of the Michael and Dieckmann reactions.

17.          What is Drug and Medicine?

18.          What are Antiseptics? Give an example with synthesis.

19.           What are Antimalarials? give two examples and any one synthesis.

20.          Explain the term 'Antibacterials' and suggest an example with synthesis.

21.          Give classification of drug according to their therapeutic uses with examples.

Assignment: 5

1.            Give synthesis and uses of Sulphanilamide, Sulphaguanidine, Chloromycetin, and Chloroquine. 

2.            Write the difference between Colour,  Dyes and Pigments.

3.            Give classification of dyes based on Application and structural representation with an example of each.

4.            What are chromophore and auxochrome explain with examples.

5.            Prepare a note on theories of colour.

6.            Write a note on application of dyes and pigments.

7.            Give preparation of dyes: Congo  red,  Malachite  Green,  Crystal  Violet, Alizarin, Phenolphthalein, Fluorescein, Eosin and Indigo.

8.            Write a note on occurrence and composition of crude oil.

9.            Explain the distillation of the Crude oil.

10.          Explain the terms:  Cracking, Knocking, Octane  Number  &  Cetane  Number.

11.          What is Synthetic petrol write any one method of preparation of synthetic petrol.

List of practicals to be performed in the Labs.

NO	TOPIC
1	To determine the melting Point of the given compound.
2	Preparation of Acetanilide from Aniline.
3	To determine flow rate of different organic compound by paper chromatography.
4	To prepare Acetylsalicylic acid from salicylic acid.
5	To synthesize Sudan‐I dye from             aniline and β‐naphthol.
6	To identify unknown organic compound.………………………..
Practicals Based on Latest Outcomes in Technology Study
7	Determination of moiture containt in given sample by Infrared moiture balance.

Assignment Submission Dates:

Sr. No	Assignments no. / Unit	Expected Date
1	Assignment:1	05-07-2017
2	Assignment:2	24-07-2017
3	Assignment:3	19-08-2017
4	Assignment:4	04-09-2016
5	Assignment:5	-10-2016

For Word file Size A4, font Times new roman: Title 14 Bold, Subtitle 13 normal, matters should be in 12 normal, All paragraphs should be justified, images should be sent as jpeg/png format sepratly with the mail, reactions and structures should be drawn in the ACD/ChemSketch software.Freeware link

File Names must be as follows : 

For word file Enrlnumber_2130501_Word.doc    example : 1234567890_2130501_Word.doc

For ppt    file Enrlnumber_2130501_PPT.ppt       example : 1234567890_2130501_PPT.ppt     PPT Format

For SAQ file Enrlnumber_2130501_SAQ.doc     example : 1234567890_2130501_SAQ.doc   SAQ Format

WORD FILE PPT,  FILE and SAQ FILE Toipcs CLICK HERE

send your file in one mail on the email ocupchem2015@gmail

Open Ended Project Title Submission: Submit your Topic of OEP Here

Mid Semester Result:

Mid-Sem Exam (SEPT-2017)  Result-OCUP (2130501)
Government Engineering College, Valsad
Department of Chemical Engineering
B.E.-3rd sem,  GTU, YEAR 2017 - 2018
Sr. No.	Enroll No.	Mid sem Marks/ 30		Sr. No.	Enroll No.	Mid Sem Marks/ 30	Sr. No.	Enroll No.	Mid Sem Marks/ 30	Sr. No.	Enroll No.	Mid Sem Marks/ 30	Sr. No.	Enroll No.	Mid Sem Marks/ 30
1	160190105001	27		31	160190105034	23	61	160190105067	27	91	160190105099	25	121	DD9	12
2	160190105002	7		32	160190105035	20	62	160190105068	19	92	160190105100	27	122	DD10	19
3	160190105003	18		33	160190105036	18	63	160190105069	22	93	160190105101	27	123	DD11	AB
4	160190105004	27		34	160190105037	21	64	160190105070	20	94	160190105102	20	124	DD12	12
5	160190105005	23		35	160190105038	19	65	160190105071	18	95	160190105103	27	125	DD13	3
6	160190105006	22		36	160190105039	18	66	160190105072	16	96	160190105104	26	126	DD14	AB
7	160190105007	26		37	160190105040	AB	67	160190105073	20	97	160190105105	21	127	DD15	4
8	160190105008	16		38	160190105041	15	68	160190105074	29	98	160190105106	12	128	DD16	13
9	160190105010	24		39	160190105043	26	69	160190105075	17	99	160190105108	27	129	DD17	10
10	160190105011	26		40	160190105045	15	70	160190105077	26	100	160190105109	16	130	DD18	4
11	160190105012	23		41	160190105046	19	71	160190105079	12	101	160190105110	19	131	DD19	15
12	160190105013	AB		42	160190105047	25	72	160190105080	19	102	160190105111	24	132	DD20	AB
13	160190105014	17		43	160190105048	29	73	160190105081	21	103	160190105112	25	133	DD21	AB
14	160190105015	29		44	160190105049	25	74	160190105082	18	104	160190105113	26	134	DD22	AB
15	160190105016	29		45	160190105050	24	75	160190105083	22	105	160190105114	25	135	DD23	AB
16	160190105017	19		46	160190105051	22	76	160190105084	13	106	160190105115	16	136	DD24	14
17	160190105018	17		47	160190105052	AB	77	160190105085	15	107	160190105116	12	137	DD25	12
18	160190105019	15		48	160190105053	18	78	160190105086	24	108	160190105117	11	138	DD26	22
19	160190105022	20		49	160190105054	14	79	160190105087	21	109	160190105118	20	139	DD27	16
20	160190105023	6		50	160190105055	16	80	160190105088	23	110	160190105119	21	140	DD28	6
21	160190105024	28		51	160190105056	4	81	160190105089	24	111	160190105120	23	141	DD29	15
22	160190105025	27		52	160190105057	5	82	160190105090	24	112	150190105057	AB	142	DD30	AB
23	160190105026	19		53	160190105058	0	83	160190105091	26	113	DD1	AB	143	DD31	9
24	160190105027	21		54	160190105060	22	84	160190105092	17	114	DD2	AB	144	DD32	6
25	160190105028	22		55	160190105061	12	85	160190105093	27	115	DD3	12	145	DD33	AB
26	160190105029	17		56	160190105062	0	86	160190105094	24	116	DD4	16	146	DD34	AB
27	160190105030	22		57	160190105063	15	87	160190105095	20	117	DD5	15	147	DD35	13
28	160190105031	25		58	160190105064	21	88	160190105096	27	118	DD6	AB	148	DD36	16
29	160190105032	18		59	160190105065	24	89	160190105097	21	119	DD7	7	149	DD37	19
30	160190105033	17		60	160190105066	25	90	160190105098	15	120	DD8	11	150

Submission Test for OCUP:2130501 October 2017