Tuesday 14 June 2016

AEI-2151302 Term Date:20-06-2016 to 21-10-2016


CUG WORKSHOP
Academic Calender

Dear students,

       Welcome to the new semester!

      I look forward to working with you over the next 18 weeks in  ADVANCED ENVIRONMENTAL INSTRUMENTATION(2151302). Get ready for a journey of a lifetime learning memories. In this class you will learn about instrumental method of chemical and pollutant analysis by optical and/or electro-analytic techniques. Some of the instruments like GC, FTIR, Spectrophotometer, TOC and many more. more over it we will learn some research and data analysis methods too. These will be useful to your shining carrier in the field of environmental science and engineering

     Weekly participation in 3 lectures and one laboratory of 4 hours are essential throughout the course to be successful in the subject. This course will have 7 Labs, 5 Hand written assignments, One power point presentation/Video Lecture collection, One active learning assignment in MS-Word file. One Open Ended Project work.

     We hope that, once more it is a good and interesting course program for you. Even though we have tried to finalize our scheduling and class rooms allocations, Class room and time changes may occur. Therefore, we would like to ask you to frequently check our notice boards for notifications and updates. It is also advised to visit this blog frequently for getting new learning experiences, learning materials or some instructions.

After learning the course you will be able to: 
-Use the instrumental method of analysis. 
-Demonstrate the ability to operate sophisticated state of art analytical instrument to quantify micro level contaminants 
-Exhibit the capability to operate and calibrate analytical instruments like TOC analyzer and GC 
-Carry out statistical analysis of the data. 

Once again welcome, and have nice learning experience. 

Useful Links of study materials

Link for Video Lectures of NPTEL

List of Experiments
NO
TOPIC



Safety Test and Safety Symbols
1
Determination of the turbidity in the given samples. 
2
Determination of flouride concentration in drinking water using spectrophotometer. 
3
To determine the iron content in commercially available vitamin tablet using spectrophotometer.
4
To separate the components of chlorophyll by ascending paper chromatography.
5
To study the thin layer chromatography (TLC).
6
Determination  of  metal  (copper)  using  Atomic  Absorption Spectrophotometer.
7
To become familiar with applications, parameters, and instrumentation used in ion chromatography 
8
To study the GC, study of influence of various operating parameters on the performance of GC.
9
Determination of TOC from wastewater using TOC analyzer


Sr. No
Assignments no. / Unit
Expected Date
Submission Date
Grade
Faculty Sign
1
Assignment:1
22-07-2016



2
Assignment:2
06-08-2016



3
Assignment:3
01-09-2016



4
Assignment:4
01-10-2016



5
Assignment:5
21-10-2016







Assignment:-1
Suggested Marks
What is Advanced Environmental Instrumentation? What is its Importance?
7

Explain the mechanism of environmental analysis
7

Write about steps of environmental analysis process
4

Give the classification of analytical methods of analysis.
7

What is the role of environmental chemist?
4

What is Electromagnetic spectrum? Explain in detail.
5

 Describe the Lambert and Beer laws of light absorption
7

Explain visual colorimetry in detail.
7

Write about instrumentation and workings of UV-Visible  spectrophotometry
7

Differentiate between spectrophotometry and colorimetry
7

Assignment:-2

Explain Working principle of Flame photometer. Which parameters can be measured using flame photometer?
7

Give the difference between Raman Spectroscopy and Infrared
Spectroscopy.
7

Write a short note on Mass Spectroscopy.
5

Explain Atomic Adsorption Spectroscopy in detail.
5

Differentiate following molecules based on IR-spectroscopy
4


 Explain in brief the importance of “Mutual exclusion rule” for the IR &Raman spectroscopy with two examples.
3


 Draw the schematic diagram of Raman-Spectrometer and describe each part in detail.
7


 Write note on infrared spectroscopy
7


 Write a note on atomic spectroscopy
5


 Write the two application of followings:
(1)UV-Visible spectroscopy(II)Infrared spectroscopy (III) Gas chromatography
6

Assignment:-3

Write the sources of Turbidity in river water. What is significance of
turbidity? And methods of determination.

7


 Write a short note on Nephelo Turbidity Meter.
7

Give the difference between visible and instrumental method for
measurement of turbidity.

4

Explain “Jackson Candle Turbidity Meter” with neat sketch.
7

Write application of turbidity data and its standard unit.



5

What is Chromatography? Explain stationary phase in Chromatography
7

Explain the working principle and operation of each unit of High Performance
Liquid Chromatograph with sketch.
7

Give the applications of High Performance Liquid Chromatography.

3

Explain the working principle and operation of each unit of gas chromatograph
with sketch. Along with its merits and demerits.
7

What is chromatography? Give the difference between stationary
phase and mobile phase in chromatography
7

Assignment:-4

Give the difference between adsorption and partition
chromatography with examples.
5


 Write the short note on “Affinity in chromatography”
3

Explain the principle of Ion Chromatography(IC) in detail

4

Explain following terminology use in chromatography
1.Normal phase 2.Reverse phase 3.Retention time 4.Retention volume 5.Relative retention 6.Column efficiency 7.Resolution
7


Explain stationary phase in Chromatography.
3


 Mention the classification of chromatography and write note on column chromatography
7


 Write a note on ion –exchange chromatography
7


 Write a note on thin layer chromatography
5


 Explain the significance of chromatography in a method of analysis
4


Word file preparation Topics and Power point presentation / video lecture collection Topics are as per the below List..


Topics for Word and PPT/video file preparation
ENROLLMENT NO Topic
140190113001 Introduction to instrumental method of analysis
140190113002 Spectroscopic Methods of Analysis: Introduction
140190113003 Electromagnetic spectrum
140190113005 Beer- Lambert law with  Applications
140190113006 Visual Colourimetry 
140190113007 UV-Visible spectrophotometry
140190113009 Infrared Spectroscopy 
140190113010 Raman Spectroscopy 
140190113011 Atomic Absorption Spectroscopy 
140190113012 Flame Emission Spectroscopy 
140190113013 Mass Spectroscopy
140190113014 Turbidimetry and nephalometry Visual method 
140190113015 Instrumental method of turbidity measurement
140190113016 Chromatography: Introduction
140190113017 Classification of chromatographic methods 
140190113018 Column Chromatography
140190113019 Liquid Chromatography 
140190113021 Adsorption Column Chromatography
140190113023 Ion exchange Chromatography
140190113024 Gas Chromatography 
140190113025 High Performance Liquid Chromatography
140190113028 Ion Chromatograph
140190113031 Partition chromatography
140190113032 Exclusion chromatography
140190113034 Elctrochromatography
140190113036 Gas Chromatography
140190113037 Inductively Coupled Plasma—Atomic Emission Spectroscopy
140190113038 Supercritical Fluid Chromatography and Extraction
140190113039 Reliability of Analytical Data and Statistical Analysis
140190113040 Electrophoresis
140190113041 Supramolecules in Solvent Extraction
140190113042 Complexometric (EDTA) Titrations
140190113044 Principles of Chromatography
140190113045 Partition Chromatography
140190113046 Sampling in Analysis
140190113047 Solvent Extraction
140190113048 Precipitation Titrations
140190113049 Polarimetry and Related Methods
140190113050 Electron Spectroscopy
140190113051 Radioanalytical Techniques
140190113052 Electroanalytical Methods: Potentiometry
140190113053 Chemical Sensors and Biosensors
140190113054 Polarography and Voltammetric Methods
140190113055 Volumetric Analysis—Acid Base Titrations
140190113058 Chemiluminescence Spectroscopy
140190113060 X-Ray Spectroscopy
140190113061 Electron Spin Resonance Spectroscopy
140190113062 Mössbauer Spectroscopy
140190113063 Atomic Fluorescence Spectroscopy
130190113033 On-line Analysers-Automated Instrumentation Methods
100110113047 Redox Titrations
110190113032 Solvent Extraction method
110190113056 Water quality parameters and standards
110193113007 Ionisation Spectroscopy
120190113010 Supramolecules in Solvent Extraction
120190113058 Thermoanalytical Methods
120193113002 Atomic Emission Spectroscopy
130190113042 Capillary Electrophoresis
120190113049 NMR Spectroscopy
Open Ended Project
Sr. No
Open Ended Project Topic
Date of final report submission
Submission Date
Grade
Faculty Sign
1

01-10-2016
Submit on the email aeibrsudani@gmail.com 


Enroll no.(s) Of Partner if any
Word file
Sr. No
Topic of MS-Word file
Date of submission
Submission Date
Grade
Faculty Sign
1


22-07-2016
Submit on the email aeibrsudani@gmail.com 


PPT file
Sr. No
Topic of MS-PPT file
Expected Date
Submission Date
Grade
Faculty Sign
1


28-07-2016
Submit on the email aeibrsudani@gmail.com 












Sort Answer Questions Assignment: Download the word file format and write questions and answers from your word file topics in the given word file format and submit by email on aeibrsudani@gmail.com. within time limit.


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